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Page 3 of 3 STEP #11 Neutralize the alcohol with sodium bicarbonate.(baking soda) Tip: When it stops fizzing you will have a neutral or slightly basic solution. STEP #12 Filter the solvent from the plant matter with the use of your funnel and filter paper. Note: If you are going to be doing a lot of oil production you should get a filter flask, aspirator and a buchner funnel. See the watchers chemistry works for information on filtering. STEP #13 Add as much water as you have alcohol/THC extract. Note: Toluene mixes with alcohol in all parts so you will not be able to separate the alcohol/toluene layers if you don’t add this water. STEP #14 Add about 1/3 as much toluene as you have alcohol/water to your flask. STEP #15 Mix all this well for about 30 seconds. Note 1: As the THC dose not want to stay in the alcohol/water layer it will move with ease into the toluene layer. STEP #16 Now use your separatory funnel to sperate the two layers. (see the watchers chemistry works for information on this procedure.) Note: The toluene/THC layer will be on top. Also the bottom layer should be a light green color. Important: If the bottom layer still has a black color you should do steps #14 to # 16 one more time, but once is usually enough. STEP #17 Evaporate the toluene/THC layer till you can no longer smell any trace of toluene. Note: when the toluene has evaporated you will have left in the bottom of your glass baking dish a black oil with a slight spice smell. Well people, there you have it the over night process for the extraction/manufacture of some of the finest hash oil anywhere.
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